8QAO
Crystal structure of TP901-1 CI-NTD89 repressor N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-21 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.8731 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 48.369, 48.369, 86.951 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.270 - 1.290 |
R-factor | 0.15111 |
Rwork | 0.150 |
R-free | 0.18288 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.026 |
RMSD bond angle | 2.296 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.480 | 1.370 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.246 | |
Rpim | 0.051 | |
Number of reflections | 46858 | 5596 |
<I/σ(I)> | 18.5 | |
Completeness [%] | 94.0 | |
Redundancy | 19.04 | |
CC(1/2) | 0.990 | 0.217 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 28% w/v PEG 4000, 0.17 M ammonium sulphate and 15% glycerol |