Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-10-23 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.033220 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 153.857, 49.506, 41.863 |
| Unit cell angles | 90.00, 98.50, 90.00 |
Refinement procedure
| Resolution | 38.860 - 1.500 |
| Rwork | 0.146 |
| R-free | 0.16280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.782 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.860 | 1.530 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.056 | 0.176 |
| Number of reflections | 47923 | 1966 |
| <I/σ(I)> | 27.9 | |
| Completeness [%] | 96.2 | |
| Redundancy | 12.8 | |
| CC(1/2) | 0.999 | 0.989 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | PEG 6000, Tris, calcium chloride dihydrate |
