8PQU
NMR structure of the Thermus thermophilus PilF-GSPIIB domain in the apo state
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE III HD | 600 | |
2 | Bruker | AVANCE NEO | 800 | |
3 | Bruker | AVANCE III HD | 700 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
10 | 1 | 1 | 3D HNCA |
11 | 1 | 3 | 2D 1H-13C HSQC aliphatic |
12 | 1 | 4 | 2D 1H-13C HSQC aliphatic |
13 | 1 | 1 | 3D HN(CO)CA |
14 | 1 | 1 | 3D HN(CA)CO |
15 | 1 | 1 | 3D HCCH-TOCSY |
16 | 1 | 1 | 3D C(CO)NH |
17 | 1 | 1 | 3D H(CCO)NH |
18 | 1 | 1 | 3D HBHA(CO)NH |
19 | 1 | 1 | 2D 1H-15N HSQC |
2 | 1 | 1 | 3D 1H-13C NOESY aromatic |
3 | 1 | 2 | 3D 1H-15N NOESY |
4 | 1 | 3 | 3D 1H-13C NOESY aliphatic |
5 | 1 | 1 | 3D HNCACB |
6 | 1 | 1 | 3D HNCO |
7 | 1 | 1 | 2D 1H-13C HSQC aromatic |
8 | 1 | 1 | 2D 1H-13C HSQC aliphatic |
9 | 1 | 1 | 3D CBCA(CO)NH |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 5.8 | AMBIENT | 318 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 20 |