8PKZ
NMR solution structure of PilF-GSPIIB in the c-di-GMP bound state
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE NEO | 600 | |
2 | Bruker | AVANCE III HD | 700 | |
4 | Bruker | AVANCE III | 950 | |
5 | Bruker | AVANCE NEO | 900 | |
7 | Bruker | AVANCE II | 600 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
10 | 1 | 1 | 3D HCCH-TOCSY |
11 | 1 | 1 | 3D HCCH-TOCSY |
12 | 1 | 1 | 2D 1H-13C HSQC aliphatic |
13 | 1 | 1 | 2D 1H-13C HSQC aromatic |
14 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
15 | 1 | 1 | 3D 1H-13C NOESY aromatic |
16 | 1 | 2 | 2D 1H-15N HSQC |
17 | 1 | 2 | 3D 1H-15N NOESY |
18 | 1 | 4 | 2D 1H-13C HSQC aliphatic |
19 | 1 | 3 | 2D 1H-13C HSQC aliphatic |
2 | 1 | 1 | 3D HNCO |
20 | 1 | 3 | 3D 1H-13C NOESY aliphatic |
21 | 1 | 5 | 2D 1H-31P-SFHMQC |
22 | 1 | 7 | 2D HNN-COSY |
23 | 1 | 6 | 2D 1H-13C HSQC aliphatic |
24 | 1 | 6 | 2D 1H-13C HSQC aromatic |
25 | 1 | 6 | 3D 1H-13C NOESY aliphatic |
26 | 1 | 6 | 3D 1H-13C NOESY aromatic |
27 | 1 | 6 | 2D 1H-15N HSQC NH2 only |
28 | 1 | 6 | 3D 1H-15N NOESY NH2 only |
29 | 1 | 6 | 2D 1H-13C HSQC aliphatic |
3 | 1 | 1 | 3D HNCA |
30 | 1 | 6 | 2D 1H-13C HSQC aromatic |
31 | 1 | 6 | 3D HCCH-COSY |
32 | 1 | 6 | 2D HCN H1'-C1'-N9 |
33 | 1 | 6 | 2D HCN H8-C8-N9 |
4 | 1 | 1 | 3D HN(CA)CO |
5 | 1 | 1 | 3D HNCACB |
6 | 1 | 1 | 3D HBHA(CO)NH |
7 | 1 | 1 | 3D C(CO)NH |
8 | 1 | 1 | 3D H(CCO)NH |
9 | 1 | 1 | 3D HCCH-COSY |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 5.8 | ambient | 318 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 20 |