8PDT
Crystal structure of Paradendryphiella salina PL7C alginate lyase soaked with dimannuronic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-08-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.799 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.710, 59.900, 88.960 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.770 - 1.090 |
R-factor | 0.1497 |
Rwork | 0.149 |
R-free | 0.17740 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.954 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.880 | 1.160 |
High resolution limit [Å] | 1.090 | 1.090 |
Number of reflections | 92201 | 14459 |
<I/σ(I)> | 7.77 | |
Completeness [%] | 98.4 | |
Redundancy | 7.16 | |
CC(1/2) | 1.000 | 0.460 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30% PEG3350, 0.1M Bis-Tris pH 5.5, 0.3M NaCl |