Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-04 |
| Detector | SIEMENS |
| Spacegroup name | P 65 |
| Unit cell lengths | 50.060, 50.060, 98.720 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 26.200 - 1.600 |
| R-factor | 0.167 * |
| Structure solution method | KNOWN |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.019 |
| Data reduction software | XENGEN |
| Data scaling software | XENGEN |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 26.200 | 1.700 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.044 * | 0.150 |
| Number of reflections | 18528 | |
| <I/σ(I)> | 20.6 | 5.8 |
| Completeness [%] | 88.0 * | 65 * |
| Redundancy | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 50MM SODIUM PHOSPHATE WITH 75% SATURATED AMMONIUM SULFATE., pH 6.5 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | 50 (mM) | ||
| 2 | 1 | 1 | ammonium sulfate | 75 (%sat) |
