8P9D
Crystal structure of p63-p73 heterotetramer (tetramerisation domain) in complex with darpin 1810 A2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.729, 113.186, 135.227 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.400 - 2.700 |
R-factor | 0.21656 |
Rwork | 0.215 |
R-free | 0.25164 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.116 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.080 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.083 | 0.848 |
Rmeas | 0.098 | 1.010 |
Rpim | 0.039 | 0.393 |
Number of reflections | 17853 | 2555 |
<I/σ(I)> | 11.8 | 2 |
Completeness [%] | 99.5 | |
Redundancy | 6 | 6.2 |
CC(1/2) | 0.998 | 0.751 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293.15 | 20% PEG3350, 0.1M bis-tris propane pH 7.0, 0.2M salicylic, sodium salt |