8P90

TARGET COMPLEX 2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-07-31
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.000
Spacegroup name	P 65 2 2
Unit cell lengths	94.657, 94.657, 441.848
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	46.280 - 2.800
R-factor	0.2718
Rwork	0.271
R-free	0.29540
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.450
Data reduction software	XDS
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.280	3.480
High resolution limit [Å]	2.740	2.740
Rmerge	0.360
Number of reflections	32276	3913
<I/σ(I)>	4.7
Completeness [%]	100.0
Redundancy	10.1
CC(1/2)		0.300

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	7.5	293	1 M LITHIUM SULFATE