8P6F

Crystal structure of PorX-Fj

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-09
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.9801
Spacegroup name	P 21 21 21
Unit cell lengths	84.609, 97.483, 131.103
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.160 - 2.000
R-factor	0.2176
Rwork	0.216
R-free	0.25490
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	0.980
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	autoBUSTER

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.110
High resolution limit [Å]	2.000	2.000
Number of reflections	73936	10652
<I/σ(I)>	8.1
Completeness [%]	100.0
Redundancy	6.7
CC(1/2)	0.998	0.319

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M Calcium Acetate, 0.1 M Sodium Cacodylate pH 6.5, 18% PEG 8000