8P6F
Crystal structure of PorX-Fj
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-09 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9801 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.609, 97.483, 131.103 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.160 - 2.000 |
R-factor | 0.2176 |
Rwork | 0.216 |
R-free | 0.25490 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.980 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | autoBUSTER |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 73936 | 10652 |
<I/σ(I)> | 8.1 | |
Completeness [%] | 100.0 | |
Redundancy | 6.7 | |
CC(1/2) | 0.998 | 0.319 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Calcium Acetate, 0.1 M Sodium Cacodylate pH 6.5, 18% PEG 8000 |