8P2N
Polymeric form of the BTB domain of ZBTB8A from Xenopus laevis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-04-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97856 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 153.695, 153.695, 153.695 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.600 - 3.100 |
R-factor | 0.2401 |
Rwork | 0.238 |
R-free | 0.26350 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.374 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (v1.20) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.600 | 3.310 |
High resolution limit [Å] | 3.100 | 3.100 |
Rpim | 0.029 | 0.751 |
Number of reflections | 11832 | 2074 |
<I/σ(I)> | 16 | 1.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 65.3 | 66.3 |
CC(1/2) | 0.999 | 0.630 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | PEG200, Na/K phosphate, NaCl |