8OV5
PERIDININ-CHLOROPHYLL-PROTEIN OF AMPHIDINIUM CARTERAE, 100K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-04 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9796 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 197.140, 115.610, 65.880 |
Unit cell angles | 90.00, 94.97, 90.00 |
Refinement procedure
Resolution | 43.380 - 1.150 |
R-factor | 0.1414 |
Rwork | 0.141 |
R-free | 0.15470 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.012 |
RMSD bond angle | 1.181 |
Data reduction software | XDS (VERSION Feb 5, 2021 BUILT=20210323) |
Data scaling software | XSCALE (VERSION Feb 5, 2021 BUILT=20210323) |
Phasing software | PHENIX (1.20.1_4487) |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.820 | 1.180 |
High resolution limit [Å] | 1.150 | 1.150 |
Rmerge | 0.044 | 0.833 |
Rmeas | 0.050 | 1.111 |
Number of reflections | 444109 | 12493 |
<I/σ(I)> | 13.33 | 1.01 |
Completeness [%] | 85.6 | 32.6 |
Redundancy | 3.5 | |
CC(1/2) | 0.999 | 0.440 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 14% PEG8000, 100mM Tris-HCL pH 7.5, 200mM MgCl2 |