8OMM
Coproporphyrin III - LmCpfC complex soaked 3min with Fe2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-05 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1.7 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.158, 67.730, 62.494 |
Unit cell angles | 90.00, 103.22, 90.00 |
Refinement procedure
Resolution | 36.170 - 2.150 |
Rwork | 0.182 |
R-free | 0.23290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.516 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.260 | 2.080 |
High resolution limit [Å] | 2.010 | 2.010 |
Number of reflections | 32898 | 1808 |
<I/σ(I)> | 7.8 | |
Completeness [%] | 99.1 | |
Redundancy | 6.5 | |
CC(1/2) | 0.997 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.3 | 293 | 17.455% PEG MME2000 0.2M Ca-Acetate 0.1M BIS-TRIS pH 6.3 |