8OI7
Trichomonas vaginalis riboside hydrolase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-11-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9724 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 92.344, 92.344, 185.111 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.321 - 1.850 |
Rwork | 0.184 |
R-free | 0.20110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.038 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.321 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Rpim | 0.027 | 0.519 |
Number of reflections | 68295 | 6037 |
<I/σ(I)> | 15.1 | 1.2 |
Completeness [%] | 98.8 | 89.1 |
Redundancy | 21.5 | 8.2 |
CC(1/2) | 0.999 | 0.625 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 90 mM PIPES pH 7.0, 90 mM MgCl2, 45 mM KCl, 1 mM NiSO4, 14% (w/v) PEG 5000 monomethyl ether |