8ODR
Mimetic of UBC9-SUMO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97856 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.280, 53.575, 100.259 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.250 - 2.850 |
R-factor | 0.2252 |
Rwork | 0.221 |
R-free | 0.25790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.504 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.250 | 3.000 |
High resolution limit [Å] | 2.850 | 2.850 |
Rpim | 0.106 | 0.506 |
Number of reflections | 6755 | 949 |
<I/σ(I)> | 5 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9 | 9.3 |
CC(1/2) | 0.982 | 0.682 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | LiSO4, Tris pH8.5, PEG 4000 |