8KFT
Crystal structure of ZmMOC1 in complex with a nicked Holliday junction soaked in Mn2+ for 15 seconds
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.978 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.280, 78.160, 63.310 |
Unit cell angles | 90.00, 98.00, 90.00 |
Refinement procedure
Resolution | 43.460 - 2.430 |
R-factor | 0.2055 |
Rwork | 0.203 |
R-free | 0.25440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6jrg |
RMSD bond length | 0.008 |
RMSD bond angle | 0.963 |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX ((1.21rc1_4958: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.430 | 2.430 |
Rmerge | 0.140 | 0.973 |
Number of reflections | 19395 | 1425 |
<I/σ(I)> | 10.1 | 2.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 6.6 | 6.9 |
CC(1/2) | 0.990 | 0.698 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 298 | 6% Isopropyl alcohol, 0.1 M Sodium acetate pH5.0, 35% Polyethylene glycol monomethyl ether 550 |