8KDK
Crystal structure of CcbF in complex with PLP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2021-11-16 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.391, 102.700, 102.954 |
Unit cell angles | 90.00, 92.44, 90.00 |
Refinement procedure
Resolution | 45.990 - 1.800 |
R-factor | 0.2037 |
Rwork | 0.203 |
R-free | 0.24750 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.976 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.990 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.108 | 0.794 |
Number of reflections | 144884 | 7101 |
<I/σ(I)> | 11.2 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.1 | 7.2 |
CC(1/2) | 0.998 | 0.751 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tris-Cl pH 8.5, 31% PEG 4000, 0.16M NaOAc |