8KCE
Structure of RvY_06210 at 1.05 angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 89.362, 64.020, 45.987 |
Unit cell angles | 90.00, 109.54, 90.00 |
Refinement procedure
Resolution | 37.020 - 1.050 |
R-factor | 0.1299 |
Rwork | 0.129 |
R-free | 0.15450 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.893 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.020 | 1.070 |
High resolution limit [Å] | 1.050 | 1.050 |
Rmerge | 0.039 | 0.576 |
Rmeas | 0.046 | 0.676 |
Rpim | 0.025 | 0.352 |
Number of reflections | 108442 | 5112 |
<I/σ(I)> | 14.9 | 1.8 |
Completeness [%] | 95.8 | |
Redundancy | 3.4 | |
CC(1/2) | 0.998 | 0.760 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Magnesium chloride hexahydrate, 0.03M Tris-HCl pH8.2 , 19% w/v PEG 4000 |