8K8M
Crystallographic structure of Lysozyme C from chicken
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-07-21 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54056 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.537, 78.537, 37.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.000 - 1.600 |
R-factor | 0.16051 |
Rwork | 0.159 |
R-free | 0.18789 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.803 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.062 | 0.583 |
Rmeas | 0.066 | 0.642 |
Rpim | 0.022 | 0.265 |
Total number of observations | 4510 | |
Number of reflections | 16043 | 784 |
<I/σ(I)> | 21.2 | 3 |
Completeness [%] | 99.8 | |
Redundancy | 8.3 | 5.8 |
CC(1/2) | 0.999 | 0.808 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 4.6 | 298 | 5%(w/v) NaCl, 0.1M Na acetate pH4.6 |