8K4R
Structure of VinM-VinL complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-17 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 56.501, 72.987, 80.209 |
Unit cell angles | 94.18, 90.87, 103.34 |
Refinement procedure
Resolution | 46.040 - 2.300 |
R-factor | 0.2089 |
Rwork | 0.207 |
R-free | 0.25080 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.445 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.370 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.049 | 0.626 |
Number of reflections | 54087 | 4443 |
<I/σ(I)> | 11.2 | 1.6 |
Completeness [%] | 97.9 | 97.3 |
Redundancy | 3.5 | 3.4 |
CC(1/2) | 0.999 | 0.826 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | HEPES-Na, sodium citrate |