8JYF
Crystal Structure of Intracellular B30.2 Domain of VpBTN3 in Complex with DMAPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | LIQUID ANODE |
Source details | BRUKER METALJET |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-03-13 |
Detector | Bruker PHOTON III |
Wavelength(s) | 1.34138 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.172, 67.895, 134.622 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.050 - 1.800 |
R-factor | 0.1724 |
Rwork | 0.170 |
R-free | 0.21630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zxk |
RMSD bond length | 0.010 |
RMSD bond angle | 1.625 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.060 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.090 | 0.351 |
Number of reflections | 38449 | 1825 |
<I/σ(I)> | 15.45 | |
Completeness [%] | 99.9 | |
Redundancy | 11.14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Bis Tris pH 5.5, 2.0 M ammonium sulfate |