8JYB
Crystal Structure of Intracellular B30.2 Domain of VpBTN3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | LIQUID ANODE |
Source details | BRUKER METALJET |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-07-02 |
Detector | Bruker PHOTON III |
Wavelength(s) | 1.34138 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.996, 68.056, 134.657 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.050 - 1.910 |
R-factor | 0.1601 |
Rwork | 0.158 |
R-free | 0.20090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zxk |
RMSD bond length | 0.011 |
RMSD bond angle | 1.659 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.050 | 1.940 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.035 | 0.115 |
Number of reflections | 32076 | 1394 |
<I/σ(I)> | 31.08 | |
Completeness [%] | 99.4 | |
Redundancy | 6.12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Bis Tris pH 5.5, 2.0 M ammonium sulfate |