8JU9
Molecular mechanism of the one-component regulator RccR on bacterial metabolism and virulence
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 74.319, 82.855, 138.622 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.660 - 2.000 |
R-factor | 0.1765 |
Rwork | 0.175 |
R-free | 0.20030 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.221 |
Data reduction software | HKL-2000 (v1.0) |
Data scaling software | HKL-2000 (v1.0) |
Phasing software | PHENIX (1.13_2998) |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.660 | 2.071 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 29112 | 2760 |
<I/σ(I)> | 25.28 | |
Completeness [%] | 99.0 | |
Redundancy | 5.2 | |
CC(1/2) | 1.000 | 0.858 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M Tris (pH 8.0), 8%PEG8000 |