8JOI
Crystal Structure of Bel-1 E166A Mutant.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-11 |
Detector | RIGAKU HyPix-6000HE |
Wavelength(s) | 1.5418 |
Spacegroup name | P 6 |
Unit cell lengths | 123.498, 123.498, 70.644 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.613 - 1.700 |
Rwork | 0.161 |
R-free | 0.22530 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.992 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.350 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.130 | |
Rmeas | 0.140 | |
Rpim | 0.050 | |
Number of reflections | 67521 | 3585 |
<I/σ(I)> | 12.2 | |
Completeness [%] | 100.0 | |
Redundancy | 13.4 | |
CC(1/2) | 0.998 | 0.773 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M imidazole, 0.1M MES monohydrate, 20% ETG, 10% PEG 8000, 0.1M Sodium formate, 0.1M Ammonium acetate, 0.1M Sodium citrate tribasic dihydrate, 0.1M Potassium sodium tartrate, 0.1M Sodium oxamate |