Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

8JIY

A carbohydrate binding domain of a putative chondroitinase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL19U1
Synchrotron siteSSRF
BeamlineBL19U1
Temperature [K]100
Detector technologyPIXEL
Collection date2023-04-08
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.979
Spacegroup nameP 21 21 21
Unit cell lengths56.313, 56.634, 69.456
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.560 - 1.550
R-factor0.1928
Rwork0.191
R-free0.22840
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle0.767
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX ((1.20.1_4487: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]43.8901.580
High resolution limit [Å]1.5501.550
Rmerge0.0560.238
Rmeas0.0620.271
Rpim0.0260.127
Total number of observations1699046887
Number of reflections327251596
<I/σ(I)>174.4
Completeness [%]99.4
Redundancy5.24.3
CC(1/2)0.9980.937
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29120% PEG 3350, 0.2 M Ammonium sulfate

227344

PDB entries from 2024-11-13

PDB statisticsPDBj update infoContact PDBjnumon