8JHW
The first crystal structure of a H-2Kb-restricted decapeptide from Cryptosporidium parvum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-11-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97915 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 86.940, 86.940, 293.730 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.359 - 3.120 |
Rwork | 0.245 |
R-free | 0.28790 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.380 | 3.340 |
High resolution limit [Å] | 3.120 | 3.120 |
Number of reflections | 12577 | 2207 |
<I/σ(I)> | 15 | |
Completeness [%] | 100.0 | |
Redundancy | 15.93 | |
CC(1/2) | 0.999 | 0.776 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 20%(w/v) Polyethylene glycol 3350; 0.2M Lithium acetate dihydrate |