8JFX
TruB domain of TruB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.315, 53.487, 90.134 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.740 - 2.200 |
R-factor | 0.2071 |
Rwork | 0.205 |
R-free | 0.24180 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.594 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.19_4092: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.000 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.091 | 0.873 |
Rmeas | 0.096 | 0.916 |
Rpim | 0.029 | 0.273 |
Total number of observations | 139128 | 12099 |
Number of reflections | 12858 | 1083 |
<I/σ(I)> | 15.5 | 2.9 |
Completeness [%] | 99.8 | |
Redundancy | 10.8 | 11.2 |
CC(1/2) | 0.998 | 0.802 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 30% PEG 2000, 0.15M Potassium bromide |