8J5I

MALT1 death domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL15A1
Synchrotron site	NSRRC
Beamline	BL15A1
Temperature [K]	103
Detector technology	CCD
Collection date	2019-12-10
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	I 2 2 2
Unit cell lengths	35.232, 83.229, 85.403
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	21.350 - 2.100
R-factor	0.2191
Rwork	0.218
R-free	0.24070
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.867
Data reduction software	HKL-2000 (HKL-2000)
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.160
High resolution limit [Å]	2.100	2.100
Rmerge	0.046	0.487
Rmeas	0.054	0.568
Rpim	0.028	0.289
Number of reflections	7761	728
<I/σ(I)>	14.8	2.98
Completeness [%]	99.2
Redundancy	3.6
CC(1/2)	0.990	1.000

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		291	PEG 3350, Tacsimate pH 6