8J48
Crystal structure of OY phytoplasma SAP05 in complex with AtGATA18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2022-11-27 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.2828 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.835, 73.397, 58.671 |
Unit cell angles | 90.00, 107.22, 90.00 |
Refinement procedure
Resolution | 36.700 - 1.940 |
Rwork | 0.202 |
R-free | 0.23650 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.700 | 2.010 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.133 | 1.006 |
Number of reflections | 20865 | 1747 |
<I/σ(I)> | 10.79 | 1.65 |
Completeness [%] | 97.2 | |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Lithium acetate dihydrate, 20% (wt/vol) polyethylene glycol 3,350 |