8J2W
Saccharothrix syringae photocobilins protein, dark state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-14 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 132.111, 97.539, 72.662 |
Unit cell angles | 90.00, 116.72, 90.00 |
Refinement procedure
Resolution | 75.180 - 1.700 |
R-factor | 0.1843 |
Rwork | 0.183 |
R-free | 0.21176 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.622 |
Data reduction software | DIALS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.180 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmeas | 0.083 | 0.953 |
Number of reflections | 90363 | 4348 |
<I/σ(I)> | 15 | 1.1 |
Completeness [%] | 99.8 | 95.9 |
Redundancy | 6.9 | 5.6 |
CC(1/2) | 1.000 | 0.700 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 38% v/v 1,4-Dioxane |