8IVL
FABP7 complexed with Cholesterol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2019-03-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.680, 54.910, 66.580 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.360 - 2.700 |
R-factor | 0.2302 |
Rwork | 0.227 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.033 |
RMSD bond angle | 1.160 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.360 | 2.800 |
High resolution limit [Å] | 2.600 | 2.700 |
Rmerge | 0.043 | 0.043 |
Number of reflections | 3750 | 357 |
<I/σ(I)> | 58.48 | |
Completeness [%] | 99.3 | |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 277.15 | 0.1 M Bis-Tris 5.5 25% w/vPEG 3350 |