8IVF
FABP7 complexed with 25-HC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2019-03-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.700, 54.110, 67.240 |
Unit cell angles | 90.00, 92.34, 90.00 |
Refinement procedure
Resolution | 42.140 - 2.600 |
R-factor | 0.2151 |
Rwork | 0.211 |
R-free | 0.24860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.027 |
RMSD bond angle | 1.492 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.140 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.043 | 0.043 |
Number of reflections | 13896 | 748 |
<I/σ(I)> | 58.48 | |
Completeness [%] | 92.9 | |
Redundancy | 19.18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.1 M Bis-Tris pH 5.5 25% w/v PEG 3350 |