8ISA
CrtMLIKE with one GsPP molecule
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.410, 59.940, 168.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.970 - 1.590 |
R-factor | 0.1764 |
Rwork | 0.175 |
R-free | 0.19940 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.986 |
Data scaling software | HKL-3000 |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.970 | 1.856 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.065 | 0.237 |
Number of reflections | 34754 | 12766 |
<I/σ(I)> | 25.49 | |
Completeness [%] | 99.1 | |
Redundancy | 12.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tris, 30% PEG 4000, 0.2M MgCl2, pH 8.5 |