8IS7

CrtMLIKE with two FsPP molecules.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-04-15
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9794
Spacegroup name	C 2 2 21
Unit cell lengths	50.338, 64.469, 171.061
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	32.230 - 1.600
R-factor	0.1772
Rwork	0.176
R-free	0.20560
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.035
Data scaling software	HKL-3000
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.630
High resolution limit [Å]	1.600	1.600
Rmerge	0.069	0.303
Number of reflections	36445	1773
<I/σ(I)>	30.75
Completeness [%]	94.1
Redundancy	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M Tris, 30% PEG 4000, 0.2M MgCl2, pH 8.5