8IS6
Apo-CrtMLIKE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-02-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.610, 64.897, 170.277 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.570 - 2.000 |
R-factor | 0.1971 |
Rwork | 0.192 |
R-free | 0.24660 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.920 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.134 | 0.481 |
Number of reflections | 19434 | 981 |
<I/σ(I)> | 49.33 | 8.3 |
Completeness [%] | 99.8 | |
Redundancy | 12.6 | |
CC(1/2) | 0.991 | 0.978 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Tris, 30% PEG 4000, 0.2M MgCl2, pH 8.5 |