8IRQ
Larimichthys crocea IFNd
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2019-01-14 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.378, 38.813, 51.091 |
Unit cell angles | 90.00, 112.82, 90.00 |
Refinement procedure
Resolution | 47.090 - 1.490 |
R-factor | 0.16447 |
Rwork | 0.162 |
R-free | 0.21890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.788 |
Data reduction software | XDS |
Data scaling software | HKL-2000 |
Phasing software | SHELXT |
Refinement software | PHENIX (v1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.090 | 1.543 |
High resolution limit [Å] | 1.490 | 1.490 |
Number of reflections | 22157 | |
<I/σ(I)> | 27.52 | |
Completeness [%] | 95.8 | |
Redundancy | 6.8 | |
CC(1/2) | 0.999 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 289.15 | PEG 2000ME, Trisbase/Hydrochloric acid |