8IRQ

Larimichthys crocea IFNd

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL02U1
Synchrotron site	SSRF
Beamline	BL02U1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2019-01-14
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	0.979
Spacegroup name	P 1 21 1
Unit cell lengths	40.378, 38.813, 51.091
Unit cell angles	90.00, 112.82, 90.00

Refinement procedure

Resolution	47.090 - 1.490
R-factor	0.16447
Rwork	0.162
R-free	0.21890
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	1.788
Data reduction software	XDS
Data scaling software	HKL-2000
Phasing software	SHELXT
Refinement software	PHENIX (v1.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.090	1.543
High resolution limit [Å]	1.490	1.490
Number of reflections	22157
<I/σ(I)>	27.52
Completeness [%]	95.8
Redundancy	6.8
CC(1/2)	0.999	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIQUID DIFFUSION		289.15	PEG 2000ME, Trisbase/Hydrochloric acid