8IQV
Asterias forbesii ferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.2915 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 116.520, 116.520, 205.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.610 - 1.910 |
R-factor | 0.2203 |
Rwork | 0.219 |
R-free | 0.24840 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.827 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.610 | 2.010 |
High resolution limit [Å] | 1.910 | 1.910 |
Number of reflections | 103947 | 103947 |
<I/σ(I)> | 6.9 | |
Completeness [%] | 99.4 | |
Redundancy | 10 | |
CC(1/2) | 0.997 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM imidazole (pH 8.0), 15%(v/v) reagent alcohol, 200 mM magnesium chloride |