8INL
LSD1 in complex with S2172
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-09-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 187.101, 187.101, 106.945 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.210 - 2.620 |
R-factor | 0.1816 |
Rwork | 0.180 |
R-free | 0.21590 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.801 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.210 | 2.740 |
High resolution limit [Å] | 2.620 | 2.620 |
Rmeas | 0.138 | 3.769 |
Rpim | 0.021 | 0.574 |
Number of reflections | 33642 | 4040 |
<I/σ(I)> | 22.3 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 40.9 | 42.8 |
CC(1/2) | 1.000 | 0.798 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1M MES (pH 6.5), 0.2M diammonium tartrate, 0.0005M TCEP, 14% PEG 3350 |