8IK5
Transcription factor LMX1a homeobox domain in complex with Wnt1 promoter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.290, 46.419, 96.098 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.077 - 1.989 |
R-factor | 0.2081 |
Rwork | 0.207 |
R-free | 0.23610 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.952 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (3.3.22) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.080 | 2.030 |
High resolution limit [Å] | 1.989 | 2.000 |
Rmerge | 0.065 | 0.607 |
Number of reflections | 14659 | 707 |
<I/σ(I)> | 33.7 | 2.3 |
Completeness [%] | 99.1 | |
Redundancy | 10.3 | |
CC(1/2) | 0.994 | 0.909 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 27% PEG MME 2000, 0.1 mM sodium cacodylate (pH 6.5) |