8IF0
NmeHNH-AcrIIC1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2017-07-18 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 93.061, 60.742, 46.428 |
Unit cell angles | 90.00, 108.25, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.570 |
Rwork | 0.193 |
R-free | 0.22900 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.738 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.610 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.092 | 0.092 |
Number of reflections | 34393 | 34393 |
<I/σ(I)> | 25.3 | |
Completeness [%] | 99.7 | |
Redundancy | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M Ammonium acetate, 0.1 M MES, pH 6.2, 26% PEG3350 |