8I7H
Meso-Diaminopimelate dehydrogenase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER D8 QUEST |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-02-20 |
Detector | Bruker PHOTON II |
Wavelength(s) | 1.541 |
Spacegroup name | H 3 2 |
Unit cell lengths | 213.300, 213.300, 245.840 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.000 - 3.020 |
R-factor | 0.20905 |
Rwork | 0.207 |
R-free | 0.24335 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.440 |
Refinement software | PHENIX (V1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.290 | 3.140 |
High resolution limit [Å] | 3.020 | 3.020 |
Number of reflections | 40836 | 4541 |
<I/σ(I)> | 8 | |
Completeness [%] | 97.0 | 96.4 |
Redundancy | 5.7 | 4.4 |
CC(1/2) | 0.980 | 0.701 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293.15 | 0.1M Sodium acetate trihydrate,2M ammonium sulfate, pH 4.5 |