8HWJ
Bacterial STING from Epilithonimonas lactis in complex with 3'3'-c-di-AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 07A |
Synchrotron site | NSRRC |
Beamline | TPS 07A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97626 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 157.171, 52.713, 88.932 |
Unit cell angles | 90.00, 114.88, 90.00 |
Refinement procedure
Resolution | 25.769 - 2.553 |
Rwork | 0.195 |
R-free | 0.22760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.438 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP (11.7.03) |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.640 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.121 | 0.578 |
Number of reflections | 20886 | 1948 |
<I/σ(I)> | 14.1 | 2.3 |
Completeness [%] | 96.5 | |
Redundancy | 6.3 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M MES pH 6.0, 0.1 M Sodium chloride, 30 % v/v PEG 3500 |