8HPE
Crystal structure of Leucine dehydrogenase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER D8 QUEST |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-14 |
Detector | Bruker PHOTON II |
Wavelength(s) | 1.54184 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 120.949, 120.949, 177.624 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.240 - 3.220 |
R-factor | 0.23571 |
Rwork | 0.233 |
R-free | 0.29529 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.527 |
Data scaling software | Aimless |
Refinement software | REFMAC (5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.200 | 3.480 |
High resolution limit [Å] | 3.220 | 3.220 |
Rmerge | 0.302 | 1.200 |
Number of reflections | 22022 | 4448 |
<I/σ(I)> | 8.7 | |
Completeness [%] | 99.9 | |
Redundancy | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% glycerol, 1.5M ammonium sulfate |