8HMH
The closed state of RGLG2-VWA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AichiSR BEAMLINE BL2S1 |
Synchrotron site | AichiSR |
Beamline | BL2S1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-06-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979183 |
Spacegroup name | P 41 |
Unit cell lengths | 62.960, 62.960, 155.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.873 - 2.560 |
R-factor | 0.1896 |
Rwork | 0.187 |
R-free | 0.24590 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.027 |
RMSD bond angle | 1.462 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.873 | 2.630 |
High resolution limit [Å] | 2.560 | 2.560 |
Number of reflections | 19226 | 962 |
<I/σ(I)> | 11.3 | 2.1 |
Completeness [%] | 99.0 | |
Redundancy | 13.9 | |
CC(1/2) | 0.994 | 0.722 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 200 mM magnesium chloride, 30% PEG 4000, 100 mM Tris-HCl, PH8.5 |