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8HBR

The C-terminal domain of Spiral2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyPIXEL
Collection date2020-06-28
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.97864
Spacegroup nameP 1 21 1
Unit cell lengths55.509, 109.560, 69.787
Unit cell angles90.00, 113.20, 90.00
Refinement procedure
Resolution40.000 - 2.200
R-factor0.2046
Rwork0.202
R-free0.25620
Structure solution methodSAD
RMSD bond length0.010
RMSD bond angle1.620
Data reduction softwareXDS
Data scaling softwarepointless
Phasing softwareCRANK2
Refinement softwareREFMAC (5.8.0352)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]46.25046.2502.230
High resolution limit [Å]2.1608.9102.160
Rmerge0.0660.0440.656
Rmeas0.0720.0480.747
Rpim0.0270.0180.347
Total number of observations261108377013291
Number of reflections403986003042
<I/σ(I)>20.659.22.3
Completeness [%]98.198.985
Redundancy6.56.34.4
CC(1/2)0.9990.9990.750
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293ammonium sulphate, BICINE (pH9)

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