8H4F
Blasnase-T13A/P55F with D-asn
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2021-10-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 92.443, 92.443, 231.509 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.820 - 1.900 |
Rwork | 0.191 |
R-free | 0.21130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7c8x |
RMSD bond length | 0.011 |
RMSD bond angle | 1.079 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (v1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.970 | 1.880 |
High resolution limit [Å] | 1.850 | 1.850 |
Rpim | 0.020 | 0.680 |
Number of reflections | 86412 | 4499 |
<I/σ(I)> | 23.6 | |
Completeness [%] | 99.9 | |
Redundancy | 20 | |
CC(1/2) | 1.000 | 0.538 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | sodium formate |