8H49
Blasnase-M57P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2021-11-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 91.674, 91.674, 231.918 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.390 - 2.000 |
Rwork | 0.191 |
R-free | 0.21370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7c8x |
RMSD bond length | 0.008 |
RMSD bond angle | 0.909 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (v1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.670 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rpim | 0.020 | 0.425 |
Number of reflections | 66776 | 4403 |
<I/σ(I)> | 19.5 | |
Completeness [%] | 98.9 | |
Redundancy | 24.9 | |
CC(1/2) | 0.999 | 0.732 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | sodium formate |