8H0J
Annexin A5 mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.987 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 69.294, 134.470, 79.227 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.630 - 2.230 |
R-factor | 0.1907 |
Rwork | 0.188 |
R-free | 0.24650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1avh |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.290 |
High resolution limit [Å] | 2.230 | 6.090 | 2.250 |
Rmerge | 0.166 | 0.106 | 1.018 |
Rmeas | 0.173 | 0.111 | 1.079 |
Rpim | 0.049 | 0.033 | 0.349 |
Number of reflections | 18237 | 998 | 884 |
<I/σ(I)> | 3.2 | ||
Completeness [%] | 100.0 | 100 | 99.8 |
Redundancy | 12.4 | 11.7 | 9 |
CC(1/2) | 0.994 | 0.699 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | PEG 3350, sodium chloride, 2-[4-(2-hydroxyethyl)piperazin-1-yl]ethanesulfonic acid |