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8GY1

Crystal structure of Ag+ binding to Dendrorhynchus zhejiangensis ferritin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNFPSS BEAMLINE BL17B
Synchrotron siteNFPSS
BeamlineBL17B
Temperature [K]100
Detector technologyPIXEL
Collection date2022-01-25
DetectorDECTRIS EIGER2 X 9M
Wavelength(s)0.979
Spacegroup nameI 4 3 2
Unit cell lengths148.212, 148.212, 148.212
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution104.800 - 1.900
R-factor0.15273
Rwork0.151
R-free0.18965
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.023
RMSD bond angle1.875
Data reduction softwareXDS
Data scaling softwareautoPROC
Phasing softwareBALBES
Refinement softwareREFMAC (ccp4-7.0.024)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]106.7802.000
High resolution limit [Å]1.9001.900
Number of reflections210033175
<I/σ(I)>7.2
Completeness [%]99.7
Redundancy11.3
CC(1/2)0.9900.920
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP4.6291.15DzFer crystals were grown in 0.2 M ammonium sulfate, 0.1 M sodium acetate trihydrate pH 4.6, 30% w/v PEG monomethyl ether 2000, followed by soaking for 10 min with 20% glycerol and 100 mM AgNO3.

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