8GXN
The crystal structure of CsFAOMT2 in complex with SAH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CAMD BEAMLINE GCPCC |
| Synchrotron site | CAMD |
| Beamline | GCPCC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-10-29 |
| Detector | DECTRIS PILATUS 300K |
| Wavelength(s) | 0.978690 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 74.688, 74.688, 81.523 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.060 - 1.340 |
| R-factor | 0.1644 |
| Rwork | 0.164 |
| R-free | 0.17080 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3c3y |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.201 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 64.740 | 1.350 |
| High resolution limit [Å] | 1.280 | 1.280 |
| Number of reflections | 61963 | 7996 |
| <I/σ(I)> | 33.6 | |
| Completeness [%] | 90.6 | |
| Redundancy | 15 | |
| CC(1/2) | 1.000 | 0.898 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 1.5M Ammonium Sulfate, 100 mM Sodium Citrate pH5.5 |
