8GS7
SOLUTION NMR STRUCTURE OF N-TERMINAL DOMAIN OF TRICONEPHILA CLAVIPES MAJOR AMPULLATE SPIDROIN 2
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 700 | |
| 2 | Bruker | AVANCE III | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC; 2D 1H-13C HSQC ALIPHATIC; 2D 1H-13C HSQC AROMATIC; 3D CBCA(CO)NH; 3D HNCACB; 3D HNCO; 3D HN(CA)CO; 3D HNHAHB; 3D HBHA(CO)NH; 3D 1H-13C NOESY ALIPHATIC; 3D 1H-15N NOESY; 3D H(CCO)NH; 3D HCCH-TOCSY; 2D HB(CBCG)CD(HD); 2D HB(CBCGCD) CE(HE) |
| 10 | 1 | 1 | 3D 1H-13C NOESY aliphatic |
| 11 | 1 | 1 | 3D 1H-15N NOESY |
| 12 | 1 | 1 | 3D H(CCO)NH |
| 13 | 1 | 1 | 3D HCCH-TOCSY |
| 14 | 1 | 1 | 2D HB(CBCGCD)CE(HE) |
| 15 | 1 | 1 | 2D HB(CBCG)CD(HD) |
| 2 | 1 | 1 | 2D 1H-13C HSQC aliphatic |
| 3 | 1 | 1 | 2D 1H-13C HSQC aromatic |
| 4 | 1 | 1 | 3D CBCA(CO)NH |
| 5 | 1 | 1 | 3D HNCACB |
| 6 | 1 | 1 | 3D HBHA(CO)NH |
| 7 | 1 | 1 | 3D HN(CA)CO |
| 8 | 1 | 1 | 3D HNCO |
| 9 | 1 | 1 | 3D HNHAHB |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7 | 1 | 298 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 20 |
